Study of global and local crystallography at the domain boundaries of Lead Zirconate Titanate piezoelectric ceramics, Artikel Nr. 012012
Farooq, MU; Villaurrutia, R; MacLaren, I; Kungl, H; Hoffmann, MJ; Freudenberger, JJ; Bouzy, E
EMAG: ELECTRON MICROSCOPY AND ANALYSIS GROUP CONFERENCE 2007; JOURNAL OF PHYSICS CONFERENCE SERIES, Band 126, S. 12012-12012
Reliable automated orientation mapping of 90 degrees domains in a tetragonal perovskite has been achieved for the first time using both EBSD and TEM-Kikuchi pattern analysis. This has been used to compare local measurements of c/a ratios in PZT with global measurements by X-ray diffraction. The local c/a rations are in broad agreement with the global measurements, but further work is needed to determine whether the small discrepancies are real local variations or are caused by experimental factors.